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Ferro Electronic Material Systems Performance of LTCC Resistors in Extreme Cold Environment Michail Moroz IMAPS ATW on Reliability of Advanced Electronic Packages and Devices in Extreme Cold Environments February 21-23, 2005 Pasadena, CA


  1. Ferro Electronic Material Systems Performance of LTCC Resistors in Extreme Cold Environment Michail Moroz IMAPS ATW on Reliability of Advanced Electronic Packages and Devices in Extreme Cold Environments February 21-23, 2005 Pasadena, CA

  2. Introduction (1) There is a growing demand for more capable extreme cold • environment electronics used in such applications as defense and aerospace systems Many space applications like exploration missions to the outer • planets, James Webb Space Telescope, earth-orbiting and deep-space probes and communications satellites, would benefit from availability of low temperature electronics Continuous interest in miniaturized, high performance and reliable • electronic devices drives the electronic industry to develop new packaging technologies In competition with alternative solutions like printed circuit board • and thin film technologies, low temperature co-fired ceramic (LTCC) technology is being developed for the fabrication of high reliability, compact, low-cost electronic modules 2

  3. Introduction (2) Most modern electronic components are limited to low operating • temperature of -40ºC to -55ºC Effect of extreme cold temperatures on the key characteristics of • resistors, specifically resistance and temperature coefficient of resistance (TCR) was investigated The following requirements were set as a goal for the present work: • � Resistivity: from 10 Ω / � to 100 K Ω / � � Resistor size range: 15x15 to 80x80 mils and 40x40 to 400x40 mils � Temperature range: from 25 ° C down to –155 ° C � TCR: within ± 100 ppm/ ° C � Relative resistivity change: < ± 1% � R 1 / R 2 ratio change for resistor pairs: < ± 0.5% 3

  4. TCR Temperature Coefficient of Resistance (TCR) – the amount of resistance • change of a resistor material with temperature TCR is also dependent on resistor geometry, resistor thickness, trimming • methods, encapsulation, and many other processing parameters Values are often quoted for "hot TCR" and "cold TCR" • Commonly expressed as the average change over a certain temperature • range in parts per million per degree Centigrade (ppm/ ° C) − ( R R ) 2 1 x 10 6 , ppm/ ° C TCR: − R ( T T ) 1 2 1 The standard TCR test uses only two readings at - 55 ° C and + 125 ° C • with reference point 25 ° C No thick film resistive inks with specified and controlled continuous • TCR curve shape for wide resistor size range are currently commercially available 4

  5. Resistor Test Pattern Resistor sizes, mils: 15x15 40x40 20x20 80x40 30x30 120x40 40x40 200x40 80x80 400x40 Pattern size: 1” x 1” 5

  6. The TCR Test System The TCR Test System enables computer-controlled • measurement of resistance and calculation of the TCR The TCR Chamber door is equipped with five • connectors that can accommodate up to 20 resistor samples The TCR Chamber is cooled by liquid nitrogen • The operator enters a series of test temperatures and dwell • time at each temperature into the system After the programmed dwell time at each temperature, the • resistance is measured for each sample The TCR is calculated for each sample using the test results at • a user defined reference temperature Test results for each test session are stored in a Microsoft • Access database and accessed using a unique test file name 6

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  11. Relative Resistivity 11

  12. TCR vs. Resistor Size in Regular Temperature Range from –55 ° C to 125 ° C 200 100 Regular Hybrid Resistor High Precision LTCC 82-31PMG Resistor 80 150 Reference Point: +25C Reference Point: +25C 60 100 40 50 TCR, ppm/°C 20 TCR, ppm 0 0 -20 -50 -40 Hot @ 125°C -100 Hot @ 125°C -60 Cold @ -55°C -150 Cold @ -55°C -80 -200 -100 40x40 80x40 120x40 200x40 400x40 40x40 80x40 120x40 200x40 400x40 Temperature, °C Temperature, °C 12

  13. TCR vs. Temperature in Standard Temperature Range from –55 ° C to 125 ° C 100 Such feature of thick High Precision LTCC 82-31PMG Resistor 80 film resistive inks like specified and 60 Reference Point: +25°C controlled continuous 40 TCR curve shape for wide resistor size 20 TCR, ppm range is very 0 desirable, as it provides significant -20 design flexibility and -40 helps to keep resistor performance precise -60 40x40 80x40 120x40 200x40 400x40 for various circuit -80 designs, facilitating -100 enhanced yield -55 -45 -35 -25 -15 -5 0 5 45 55 65 75 85 95 105 115 125 during manufacturing Temperature, °C 13

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  15. New High Precision LTCC Resistor Regular Resistor < ±100 ppm°C @ -55°C 15

  16. New High Precision LTCC Resistor Regular Resistor < ±100 ppm°C @ -55°C 16

  17. TCR in the Temperature Range from 25 ° C to -155 ° C for 20x20 mils Resistors 100 Reference Point: +25°C 50 0 -50 TCR, ppm/°C -100 -150 20 x 20 mils Resistors -200 High Precision 82-51PMG Resistor -250 Regular ± 100 ppm/°C Resistor -300 -350 5 5 5 0 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 - 1 2 3 4 5 6 7 8 9 0 1 2 3 4 5 2 1 - - - - - - - - - 1 1 1 1 1 1 - - - - - - Temperature, °C 17

  18. Relative Resistivity Change in the Temperature Range from 25 ° C to -155 ° C (20x20 mils size) 1.00 0.50 0.00 Relative Resistivity Change, % -0.50 -1.00 -1.50 -2.00 -2.50 Reference Point: +25°C -3.00 -3.50 20 x 20 mils Resistors -4.00 -4.50 High Precision 82-51PMG Resistor -5.00 Regular ± 100 ppm/°C Resistor -5.50 -6.00 5 5 5 0 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 2 1 - 1 2 3 4 5 6 7 8 9 0 1 2 3 4 5 - - - - - - - - - 1 1 1 1 1 1 - - - - - - Temperature, °C 18

  19. TCR in the Temperature Range from 25 ° C to -155 ° C 100 100 Regular Hybrid Resistor High Precision LTCC 82-31PMG Resistor 50 80 60 0 40 -50 TCR, ppm/°C TCR, ppm/°C 20 -100 0 -150 40X40 -20 -200 80X40 -40 Reference Point: +25°C 120X40 -250 200X40 -60 Reference Point: +25°C -300 400X40 40X40 80X40 120X40 200X40 400X40 -80 -350 -100 5 5 5 0 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 2 1 - 1 2 3 4 5 6 7 8 9 0 1 2 3 4 5 - - - - - - - - - 1 1 1 1 1 1 25 15 5 0 -5 -15 -25 -35 -45 -55 -65 -75 -85 -95 -105 -115 -125 -135 -145 -155 - - - - - - Temperature, °C Temperature, °C For extreme temperature applications continuous TCR curve with a controlled slope is a newly introduced, but mandatory requirement 19

  20. Relative Resistivity Change in the Temperature Range from 25 ° C to -155 ° C 1.00 1.00 Regular Hybrid Resistor High Precision LTCC 82-31PMG Resistor 0.50 0.80 0.00 Relative Resistivity Change, % 0.60 -0.50 Relative Resistivity Change, % -1.00 0.40 -1.50 0.20 -2.00 -2.50 0.00 40X40 -3.00 80X40 -0.20 -3.50 Reference Point: +25°C 120X40 -4.00 -0.40 200X40 -4.50 -0.60 400X40 -5.00 Reference Point: +25°C 40X40 80X40 120X40 200X40 400X40 -5.50 -0.80 -6.00 -1.00 0 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 2 1 - 1 2 3 4 5 6 7 8 9 0 1 2 3 4 5 - - - - - - - - - 1 1 1 1 1 1 - - - - - - 25 15 5 0 -5 -15 -25 -35 -45 -55 -65 -75 -85 -95 -105 -115 -125 -135 -145 -155 Temperature, °C Temperature, °C 20

  21. R 1 /R 2 Ratio of Resistor Pair Quite often pairs of resistors are used in circuit design when • R 1 / R 2 ratio is even more important than their absolute values If two resistors with a different number of squares are used, and • one resistor is changing TCR faster than the other (i.e. has a different TCR curve slope), this would be an indication the R 1 / R 2 ratio is not at –155 ° C as accurately as with the standard temperature range of –55 ° C For the pair consisting of same-width 10-square and 1-square • precise regular resistors with TCR ± 100 ppm/ ° C at –55 ° C, the R 1 / R 2 ratio change at –155 ° C was as high as -2.5% The R 1 / R 2 ratio change for the specifically designed 82-series • LTCC post fired resistors did not exceed ± 0.2% at -155 ° C for any resistor configuration 21

  22. R 1 /R 2 Ratio Change in the Temperature Range from 25 ° C to -155 ° C 1.00 1.00 High Precision LTCC 82-31PMG Resistor Regular Hybrid Resistor 0.80 0.50 Reference Point: +25°C 0.60 Reference Point: +25°C 0.00 0.40 R1 / R2 Change, % R1 / R2 Change, % -0.50 0.20 0.00 -1.00 400x40 / 40x40 -0.20 -1.50 400x40 / 40x40 400x40 / 80x40 -0.40 -2.00 400x40 / 80x40 400x40 / 120x40 -0.60 400x40 / 120x40 -2.50 -0.80 400x40 / 200x40 400x40 / 200x40 -3.00 -1.00 25 15 5 0 -5 -15 -25 -35 -45 -55 -65 -75 -85 -95 -105 -115 -125 -135 -145 -155 25 15 5 0 -5 -15 -25 -35 -45 -55 -65 -75 -85 -95 -105 -115 -125 -135 -145 -155 Temperature, °C Temperature, °C 22

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