A Novel Approach to Handling & Dispensing A Novel Approach to Handling & Dispensing A Novel Approach to Handling & Dispensing A Novel Approach to Handling & Dispensing . High Purity Solvents in the Working Lab . High Purity Solvents in the Working Lab High Purity Solvents in the Working Lab High Purity Solvents in the Working Lab For : Western Canada For : Western Canada For : Western Canada Trace Organic Workshop Trace Organic Workshop Trace Organic Workshop Brian Finniss Brian Finniss Brian Finniss Gerry Chin Pang Gerry Chin Pang Gerry Chin Pang
Overview Overview Overview Overview � 35 year old Canadian company, located in Georgetown, 35 year old Canadian company, located in Georgetown, � Ontario. Ontario. � Full spectrum chemical supplier. (Acids, solutions, chem.) Full spectrum chemical supplier. (Acids, solutions, chem.) � � Renowned for high purity solvents for HPLC, GC, GC/ MS. Renowned for high purity solvents for HPLC, GC, GC/ MS. � � Distribute for Chiron, Chem Service, SPE Distribute for Chiron, Chem Service, SPE X/ Protocol, � X/ Protocol, Alconox, Inorganic Ventures. Alconox, Inorganic Ventures. � E E xporters to China, Malaysia, Taiwan, Mexico, Middle E ast. xporters to China, Malaysia, Taiwan, Mexico, Middle E ast. � � Contract supplier for the Ontario Govt. Labs. Contract supplier for the Ontario Govt. Labs. � • • Lot Segregation Lot Segregation • Recycling and Re- -use of solvent bottles and cartons use of solvent bottles and cartons • Recycling and Re
Overview of Semi bulk containers Overview of Semi bulk containers Overview of Semi bulk containers Overview of Semi bulk containers The Caledon semi bulk solvent container program (SBSC) � The Caledon semi bulk solvent container program (SBSC) � provides a safe , economical and environmentally responsible provides a safe , economical and environmentally responsible method of delivering larger quantities of high purity solvents to o method of delivering larger quantities of high purity solvents t the point of use. the point of use. Solvents packaged in stainless steel returnable containers. 4l, � � Solvents packaged in stainless steel returnable containers. 4l, 18L., 200L., 1250L.. 18L., 200L., 1250L.. � Fittings and hardware designed to dispense to a fume hood or to Fittings and hardware designed to dispense to a fume hood or to � a lab a lab Available in 15 PSI or 50 PSI configuration � Available in 15 PSI or 50 PSI configuration �
Features & Benefits Features & Benefits � Reduces storage for bottles Reduces storage for bottles � � 200 litre containers 200 litre containers � � No noise pollution No noise pollution � � No pumps involved No pumps involved � � Reduces hazards Reduces hazards � � Nitrogen pressured dispense Nitrogen pressured dispense � � Maintain flow rate Maintain flow rate � � Control valve inlet/ outlet Control valve inlet/ outlet � � Reduces accidental spills, Reduces accidental spills, � � Closed system Closed system � toxic fumes toxic fumes � Bottle transport Bottle transport � � Minimizes personnel Minimizes personnel � handling handling � Batch consistency Batch consistency � � Integrity of quality Integrity of quality � � Reduced packaging Reduced packaging � material material
SBSC 215L container SBSC 215L container
-side view side view SBSC container- SBSC container
Applications Applications- -who is using it? who is using it? who is using it? Applications Applications who is using it? Pharmaceutical companies companies � Pharmaceutical � � Specialty manufacturing companies Specialty manufacturing companies � � Custom project manufacture Custom project manufacture � � Research and Q.C. Research and Q.C. � � Biotechnology companies Biotechnology companies � � E E nvironmental labs nvironmental labs �
Specifications Specifications Specifications Specifications � CRN registration # L8424.5 CRN registration # L8424.5 � � ASME ASME certified for 50 PSI (MAWP) certified for 50 PSI (MAWP) � � Rupture disc blows at 56 PSI Rupture disc blows at 56 PSI � � Typical operating pressure ranges from 0 Typical operating pressure ranges from 0- -50PSI 50PSI � � Tanks are UN and DOT approved for storage and Tanks are UN and DOT approved for storage and � transport of flammable liquids transport of flammable liquids � Tanks and connectors are color coded Tanks and connectors are color coded �
Technical Specifications Technical Specifications Technical Specifications Technical Specifications � Height: Height: 55.125ins (1.4m) 55.125ins (1.4m) � � Diameter : Diameter : 22.0ins(56cms) (56cms) 22.0ins � � Container body: Container body: 304 stainless ASME SA240 304 stainless ASME SA240 � � Internal container finish: Internal container finish: electropolished electropolished � � Container wall thickness: 0.079ins (2mm) Container wall thickness: 0.079ins (2mm) � � Capacity: Capacity: 215L 215L � � Fill Volume: Fill Volume: 200L 200L � � Tare weight: Tare weight: ~150lbs (~70kgs) ~150lbs (~70kgs) � � Working Pressure: Working Pressure: 50PSI 50PSI � � UN Code: 1A1/ X2.0/ 620/ 96/ USA/ M4471/ 2.0MM UN Code: 1A1/ X2.0/ 620/ 96/ USA/ M4471/ 2.0MM �
SBSC Valve fittings SBSC Valve fittings
Technical Specifications Technical Specifications � Container working Pressure Container working Pressure 45PSI 45PSI � � Fork truck channels Fork truck channels 3.9” H x 8.5” W x 22’ D 3.9” H x 8.5” W x 22’ D � � Valves Valves Swagelok pack- -less less Swagelok pack � diaphragm diaphragm � Gas Pressurization connect Gas Pressurization connect Swagelok QT2 (keyless) � Swagelok QT2 (keyless) � Liquid Connect Liquid Connect Swagelok QT2 or QT4 Swagelok QT2 or QT4 � � Pressure gauge Pressure gauge -3.0”Hg 3.0”Hg- - 100psi 100psi � - compound compound
Top View of SBSC Top View of SBSC
Pricing Pricing Pricing Pricing � Outright purchase of SBSC units from Outright purchase of SBSC units from � manufacturer at $3,300.00US each manufacturer at $3,300.00US each � 5 Year rental option through Caledon 5 Year rental option through Caledon- - $167.00/ $167.00/ � month per unit month per unit � 5 year lease to OWN option through Caledon 5 year lease to OWN option through Caledon- - � $175.00/ month per unit $175.00/ month per unit � In both cases units remain the property of In both cases units remain the property of � Caledon until end of 5th year Caledon until end of 5th year
Chemicals Available With this Program Chemicals Available With this Program Chemicals Available With this Program Chemicals Available With this Program � Acetone Acetone � � Acetonitrile Acetonitrile � � Dichloromethane Dichloromethane � � E E thyl E ther thyl E ther � � Hexane Hexane � � Methanol Methanol � � 2 2- -Propanol Propanol � � Tetrahydrofuran Tetrahydrofuran � � Toluene Toluene �
SBSC , Valve connections,piping to Lab Instrument SBSC , Valve connections,piping to Lab Instrument
Now- -Pak HDPE Pak HDPE with Teflon Now with Teflon � HDPE HDPE outer outer � � Teflon inner Teflon inner �
Features of HDPE / Teflon lined Features of HDPE / Teflon lined � Liners made in Class 10/ 100 clean room Liners made in Class 10/ 100 clean room � � Liner material free of pigments, adhesives Liner material free of pigments, adhesives � additives and stabilizers additives and stabilizers � Safe double containment design Safe double containment design � � Reusable recyclable overpacks Reusable recyclable overpacks � � DOT/ UN approved containers DOT/ UN approved containers � � Multiple dispense connector options Multiple dispense connector options �
Now Pak connectors Now Pak connectors � Stainless steel outer Stainless steel outer � � Teflon inner Teflon inner � � Teflon connector Teflon connector �
NOWPAK- -Teflon lined with Connector Teflon lined with Connector NOWPAK
Benefits of Teflon/ HDPE containers Benefits of Teflon/ HDPE containers � Compatibility Compatibility- -universal compatibility with solvents and universal compatibility with solvents and � reagents reagents � Ultra pure Ultra pure- -metal free and low organic extractable metal free and low organic extractable � performance performance � Reduced costs Reduced costs- -single use liner eliminates cleaning, single use liner eliminates cleaning, � traceability and validation costs traceability and validation costs � Increased storage space Increased storage space- - 60% more efficient than bottles 60% more efficient than bottles � � Packaging waste reduction Packaging waste reduction- -generates 75% less waste generates 75% less waste � � Improved Lab safety Improved Lab safety- - reduces exposure of personnel to reduces exposure of personnel to � toxic fumes toxic fumes
Totes stainless steel - -1000L 1000L Totes stainless steel
Top View of 1000L Tote Top View of 1000L Tote
Totes stainless steel - -2000L 2000L Totes stainless steel
Tote – –bottom outlet connector bottom outlet connector Tote
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