AW Central Lab - UCMR 3 Sampling Protocols Sampling Protocols - PowerPoint PPT Presentation

AW Central Lab - UCMR 3 Sampling Protocols Sampling Protocols Presenter: Cody Cruse Rev 01-22-13 Rpt Ver: andy 1/22/2013 2:23:35 PM 1 of 17

Agenda • Review UCMR 3 Test Groups • Sampling Protocols • Storage and Transportation 2 Rpt Ver: andy 1/22/2013 2:23:35 PM 2 of 17

UCMR 3 Test Groups and Methods • List 1 – Assessment Monitoring (AM): § 200.8 – Metals (5) § 218.7 – Hexavalent Chromium § 300.1 – Chlorate § 522 – Dioxane § 524.3 – VOCs (7) § 537 – Perfluorinated Compounds (6) § 537 – Perfluorinated Compounds (6) • List 1 DSMRT – Assessment Monitoring (AM): § 200.8 – Metals (5) § 218.7 – Hexavalent Chromium § 300.1 – Chlorate • List 2 – Screening Survey (SS): § 539 – Hormones (7) 3 Rpt Ver: andy 1/22/2013 2:23:35 PM 3 of 17

List 1 Containers 537 FB 522 Transfer Samples 537 524.3 Containers FBs FBs 200.8 FB 522 537 524.3 200.8 218.7 300.1 Field Samples Samples Sample Sample Sample Pres 4 Rpt Ver: andy 1/22/2013 2:23:35 PM 4 of 17

List 2 Containers 539 FB 539 539 Transfer Samples FBs Containers 5 Rpt Ver: andy 1/22/2013 2:23:35 PM 5 of 17

List 1 DSMRT Containers 200.8 FB 200.8 218.7 300.1 Sample Sample Sample 6 Rpt Ver: andy 1/22/2013 2:23:35 PM 6 of 17

UCMR 3 – Special Sampling Protocols • Collect on the 2 nd Tuesday of the Month • Nitrile gloves must be worn during collection – three pairs provided in kits (sizes M, L, XL) • Collect from spigot, faucet or tap • Remove aerators and recommend removing hoses • No direct contact or breathing over samples (539) • No direct contact or breathing over samples (539) • Field preservation addition (522) • Field Blanks – Three types: § 200.8 – Break seal, open, re-cap and return § 524.3 – Do not open and return § 537 & 539 – Break seal, open, transfer to FB container, re-cap and return all containers 7 Rpt Ver: andy 1/22/2013 2:23:35 PM 7 of 17

Method 522 Field Preservation (List 1) 1) Un-cap, fill with sample, re- cap and invert to dissolve pre-preservative 2) Un-cap and add field preservative 3) Re-cap and return to the lab Nitrile Gloves Field preservative 8 Rpt Ver: andy 1/22/2013 2:23:35 PM 8 of 17

Method 200.8 Field Blank (List 1 and List 1 DSMRT) 1) Break seal and open FB at sampling location 2) Wait 5 seconds Nitrile 3) Re-cap and return to the lab Gloves 9 Rpt Ver: andy 1/22/2013 2:23:35 PM 9 of 17

Method 524.3 Field Blank (List 1) 1) Transport to sampling location 2) Do Not Open 3) Return to the lab 10 Rpt Ver: andy 1/22/2013 2:23:35 PM 10 of 17

Method 537 Field Blank Transfer Process (List 1) 1) Break seal and open FB containers at sampling location 2) Transfer contents 3) Re-cap and return all containers to the lab Nitrile Gloves 11 Rpt Ver: andy 1/22/2013 2:23:35 PM 11 of 17

Method 539 Field Blank Transfer Process (List 2) 1) Break seal and open FB containers at sampling location 2) Transfer contents 3) Re-cap and return all containers to the lab Nitrile Gloves 12 Rpt Ver: andy 1/22/2013 2:23:35 PM 12 of 17

UCMR 3 – Storage and Transportation • Collect on the 2 nd Tuesday of the month • Pack cooler with frozen ice packs • Deliver kits to Suburban Labs same day as collection 13 Rpt Ver: andy 1/22/2013 2:23:35 PM 13 of 17

List 1 Kit Shipment 14 Rpt Ver: andy 1/22/2013 2:23:35 PM 14 of 17

List 1 and List 1 DSMRT Kit Shipment 15 Rpt Ver: andy 1/22/2013 2:23:35 PM 15 of 17

List 2 Kit Shipment 16 Rpt Ver: andy 1/22/2013 2:23:35 PM 16 of 17

Thank You Rpt Ver: andy 1/22/2013 2:23:35 PM 17 of 17