Research @ Elettra - Sincrotrone Trieste Elett ettra ra Labora - PowerPoint PPT Presentation

Research @ Elettra - Sincrotrone Trieste Elett ettra ra Labora rato tory ry Mission: n: Using ng Sync nchrotron hrotron and d FEL L radiat diation ion to o con onduc duct t experi riments ments con onside sidered red impossi ssibl ble a decade cade ago o ! ELETTRA ELETT RA Maya ya Kiskin inova ova 7 th ILSF Users’ Meeting, Tehran 20 -21 April 2015

Elettra-Sincrotrone Trieste: http://www.elettra.eu Multid idisci ciplin plinary ary intern rnational ational labor oratory atory of excelle llence ce, special cialized ized in synchro rotro tron and free-electron electron laser er radi diatio ations ns and their ir appl plicati ication ons. s. Alf lfons onso o Franc ancios iosi President and Chief Executive Officer Maya ya Kiskin inova ova 7 th ILSF Users’ Meeting, Tehran 20 -21 April 2015

Industrial Liaison Office (ILO): activities using the skills and know-how of the beamline and machine scientists who are consulting ILO and also execute service when requested Solaris Synchrotron – Krakow (PL) Elettra: to be operated 550-1.5 GeV  Provides consulting in design, installation, test and commissioning tasks;  Design, manufacturing, and delivery with installation and site acceptance test of the complete UARPES Beamline € 3.070.000 (to be completed by April-May 2015);  Training scientists . Elettra involved in:  Producing 4 improved RF cavities ~ 1.4 mln  Train SESAME personnel Maya ya Kiskin inova ova 7 th ILSF Users’ Meeting, Tehran 20 -21 April 2015

High quality insertion device for light sources: http://www.kyma-undulators.eu Scientific backup by Elettra Sincrotrone Trieste Fabrication of insertion devices for light sources combining more than twenty years experience in design, assembling, characterization and operation of insertion devices at Elettra- Sincrotrone Trieste and Fermi, with the manufacturing capabilities of the industrial partners and shareholders. Maya ya Kiskin inova ova 7 th ILSF Users’ Meeting, Tehran 20 -21 April 2015

Kyma and Cornell University are cooperating under an exclusive license agreement for the design, realization and commercialization of low cost high-performance compact undulators, based on new concepts Fixed-gap, variable-phase, compact LPUs Maya ya Kiskin inova ova 7 th ILSF Users’ Meeting, Tehran 20 -21 April 2015

ELETTRA Storage Ring Fermi -FEL 23 operating BLs, 2 under commissioning 3 operating beamlines, 3 under construction FEL1: 20 – 70 nm FEL2: 4-20 nm n = c/ l % coherent polarised tunable Transient gratings, generated by the interference of coherent extreme-ultraviolet pulses delivered by the FERMI free-electron laser Operating at 2.0 Nature 520, 205 (2015), DOI:10.1038/nature14341 and 2.4 GeV October 6, 2014: INAUGURATION IAEA-Elettra XRF beamline Maya ya Kiskin inova ova 7 th ILSF Users’ Meeting, Tehran 20 -21 April 2015

Laboratories backing the scientific and training activity of the Elettra and Fermi beamlines User support lab Collaboration with University Workshop and sample preparation Trieste for training students in tools incl. chemical laboratory. Synchrotron environment. MUST Complementary research to PES and XAS beamlines (SuperESCA, NanoSpec, VUV etc ) Structural Biology lab Molecular and structural biology Powder Diffraction tools to complement research Support laboratory for MCX, XRD using SAXS and XRD beamlines . and XAFS beamlines Tomolab NanoInnovation Laboratory Complementary to the SYRMEP Atomic Force Microscopy for complementary beamline setup for micro-CT studies in support of all beamlines. with microfocus lab source Micro and Nano Carbon Lab: Scientific Computing off-line laboratory for samples Beamline Controls, Data acquisition, management and processing preparation and analysis focused on C MUST materials and sensor related research, CITIUS and T-ReX Laser labs complementing Fermi and slicing source experiments. CITIUS is located in the near-by University of Nova Goriza in Slovenija Maya ya Kiskin inova ova 7 th ILSF Users’ Meeting, Tehran 20 -21 April 2015

Beamtime at ELETTRA and FERMI@Elettra: via proposals judged for scientific merits by independent PRPs Italy 39% 443 got beamtime Average overbooking ≈ 2 – some beamlines > 3! Maya ya Kiskin inova ova 7 th ILSF Users’ Meeting, Tehran 20 -21 April 2015

BL 10. 1 X Ray Fluorescence beamline The XRF beamline can host two stations. The first is the IAEA multi-purposes station (UHVC-PTB Berlin) combining different XRF techniques: total reflection XRF, grazing incidence XRF, XANES. Partly operational for users in 2015 with 40% beamtime for IAEA users and training activities. Maya ya Kiskin inova ova 7 th ILSF Users’ Meeting, Tehran 20 -21 April 2015

First results obtained by users at BL 10. 1 X Ray Fluorescence Zn distribution and speciation Air Particulate Localization and speciation of Hg in edible Matter collected in Bangladesh mushrooms K. Vogel- Mikuš et al, Uni Ljubliana, Slo Black Glaze Fe-based decorations of Ancient ceramics: pre-edge XANES P. Romano et al, INFN, Catania (420- 400 b.C.) These first results were obtained in the frame IAEA Coordinated Research Project (CRP) program for scientists from associated countries and during the first training course for Asia-Pacific Countries in November 2014. Maya ya Kiskin inova ova 7 th ILSF Users’ Meeting, Tehran 20 -21 April 2015

Austrian SAXS beamline: one of the most productive beamlines New Detector and upgrade program ongoing . The quality of a new class of Characterization crystal Metal organic frameworks (MOF) - ultraporous luminescent structure (GIXRD) and very promising ultra-porous materials for materials probed with (SAXS): the morphology (GISAXS and a variety of applications, such as diffraction results confirm the XRR) of the magnetron sensing, detecting, gas storage and crystalline order of the framework sputtered W films as a separation catalysis and drug delivery. matrix surrounding the QDs. function of Ar pressure and sputter power Structural Characterization of MOF-5 crystals allowing for dynamic positioning in a magnetic field Maya ya Kiskin inova ova 7 th ILSF Users’ Meeting, Tehran 20 -21 April 2015

SYRMEP Mammography with Synchrotron Radiation: First Clinical Experience with Phase-Detection Technique, Radiology. 2011 Jun;259(3):684-94 Lungs imaging @ SYRMEP complements optical fluorescence microscopy visualizing Ba- labeled macrophages trafficking to inflammation sites Since December 2014 under discussion new project with in the field of Tomography and XRF using white light as well. Ongoing ERIC project application for bio-imaging Bones Ba (Mancini-Tromba) Sample: acute asthma mouse treated with macrophages labeled with Ba Application of Phase Retrieval  Reducing noise and artefacts around the tissue edges;  Enhancing the phases separation; asthmatic mouse Healthy Ba treated Healthy untreated Maya ya Kiskin inova ova 7 th ILSF Users’ Meeting, Tehran 20 -21 April 2015

Adding spin filtered momentum detection in XPEEM microscope @ NanoESCA Photon energy 50 eV Spin resolved Fermi surface of Co (10ML Co/Cu(100) Spin polarization map spin integrated intensity C. Tusche et al., Ultramicroscopy 130, 70 (2013)  aberration corrected energy filter;  spin filtering by reflection at W(100) mirror FZJ, Peter Grünberg Institute – Prof. C. Schneider Max-Planck-Institut für Mikrostrukturphysik, Halle – Prof. J. Kirschner C. Tusche et al. Ultramicroscopy 130, 70-76 (2013) The set-up allows for mapping the intensity distribution of the photoelectrons emitted into the complete solid angle as a function of the momentum component parallel to the surface, within a single image acquisition and spin resolution. Upgrade to energy resolution < 50 meV. To be open for users second semester of 2015. Maya ya Kiskin inova ova 7 th ILSF Users’ Meeting, Tehran 20 -21 April 2015

APE beamline: combining sample fabrication and characterization with conventional and synchrotron-based methods Omicron EA125 APE-HE Variable polarization photons 150-1600 eV Distribution center Users’ docking ports S segregation STM on Fe(100)  Growth facilities (oxide MBE + new preparation chamber); Load-lock  In-operando XAS/XMCD/XLMD/XPS; MO Kerr effect; LEED/Auger  Integration of spin-polarization measurements with ARPES; Sample growth and prep.  Ultrafast spectroscopy; Sample preparation  Information management and data repository; APE-LE Variable polarization Fe(100) photons 8-120 eV Fermi surface VG-Scienta DA30 Maya ya Kiskin inova ova 7 th ILSF Users’ Meeting, Tehran 20 -21 April 2015

Publications 2014: increasing trend in number and % with high impact factor publications 2014: 47% IF > 7 2014 2013 2012 Maya ya Kiskin inova ova 7 th ILSF Users’ Meeting, Tehran 20 -21 April 2015

APE Beamline: Electrical and reversible on/off switching of the interfacial FeO x magnetization in the Fe/BTO heterostructure G. Radaelli et al. 5, 3404 (2014) By performing XMCD experiment while applying an electric bias it was possible to discover a ferromagnetic-antiferromagnetic phase transition in the Fe oxide layer at the Fe/BTO interface as a function of the BTO electrical state. The yellow stripe indicates the energy region, corresponding to the Fe oxide where XMCD changes (dichroic effect) can be supp a function of the BTO electrical poling. Maya ya Kiskin inova ova 7 th ILSF Users’ Meeting, Tehran 20 -21 April 2015