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Infrared Detection of Defects in Green-State and Sintered PM Compacts Souheil Benzerrouk Reinhold Ludwig Worcester Polytechnic Institute October 27-28, 2004 M orris B oorky P owder M etallurgy R esearch C enter 1 A warm Welcome from Prof.


  1. Infrared Detection of Defects in Green-State and Sintered PM Compacts Souheil Benzerrouk Reinhold Ludwig Worcester Polytechnic Institute October 27-28, 2004 M orris B oorky P owder M etallurgy R esearch C enter 1

  2. A warm Welcome from Prof. Ludwig 2

  3. Research Objectives  Evaluate the feasibility of IR imaging for the detection of surface and subsurface defects in P/M parts  Establish a full dynamic thermo-electric IR solution that allows the testing of both green state and sintered P/M parts  Estimate experimentally effects from equipment radiation in a manufacturing environment 3

  4. Research Approach  Establish the necessary background in the fields of radiation, imaging and detection  Construct a dynamic test bed to test for subsurface defects  Test Controlled samples with subsurface defects  Process evaluation through on-line testing of P/M parts 4

  5. Outline  IR imaging: sources of radiation  Test Arrangement  Experimental study: subsurface defects imaging and data processing  Experimental Study: on-line testing of green state parts  Accomplishments  Future work 5

  6. IR imaging Signal processing computer DC power supply Incident radiation from the Sample surroundings under test Reflected radiation Contacts Emitted radiation Radiation from the IR camera surroundings  Sources of radiation S S S S = + + Incident from the sample s r at  Reflected  Atmospheric  6 Generic Formulation

  7. Test Arrangement  DC Power supply Signal processing computer  Motorized press DC power supply system GPIB  An IR camera at Switch Firewire Function 0.3m away from the generator sample under test Sample under test Contacts  A computer for IR camera processing and camera controls 7 Test Arrangement

  8. Test Arrangement Control computer Press  A switching circuit, system for pulse shaping Painted P/M part and synchronous DC Power IR camera operation supply Switching circuit 8 Test Arrangement

  9. Subsurface Defects  Part parameters:  Green state part with pure iron: 1000B Current  No lubrication step  Defect:  Location:2 mm from the surface, 2.5 cm from the top  1 mm hole 9 Experimental Results

  10. Subsurface Defects: Processing 10 Experimental Results

  11. Subsurface Defects: Processing Spot Temperature Over Time 303.4 Signature from the subsurface defect 303.2 303 Temperature (Kelvin) 302.8 302.6 302.4 302.2 302 0 5 10 15 20 11 Experimental Results

  12. Transient Model: Reminder t =0.2 sec Current step t =1 sec 12 2D Study and Sensitivity Estimation

  13. Transient Model: Reminder  Surface and subsurface defects are easily detected  Fast response, very efficient, suitable for a go/no go test  Highly sensitive, reduced post-processing complexity  Camera requirements include:  Dynamic range: 2 Hz  Thermal sensitivity: 0.2 0 C 13 2D Study and Sensitivity Estimation

  14. Subsurface Defects: New Samples Parts courtesy of Nichols Portland Part Parameters:  Density: 7.2 g/cc  Material: FC0205  Lubricant: 0.55% EBS  Embedded Defects:  Material: Glass bead  Size: 0.8mm  14 Experimental Results

  15. Subsurface Defects: New Samples Parts courtesy of Nichols Portland 15 Experimental Results

  16. Subsurface Defects: Discussion  Method successful in the detection of subsurface defects  Thermal signature is dependent on defect size, shape, orientation and distance from the surface: Diffusion  Smaller defects or deeply imbedded defects (distance from the surface is greater than the size of the defect) require a stable background and a sensitive detector 16 Experimental Results

  17. On-Line Testing  Requirements:  Fast response  High spatial resolution  High temperature range  High image recording rate  Benefits:  Allows 100% testing  Provides real time feedback on part quality and process repeatability 17 Experimental Results

  18. On-Line Testing  Part Constituents:  FLC-4608  0.9% graphite content  0.75% KENOLUBE P-11 Lubricant  Manufacturing rate: 500parts/hour Parts courtesy of GKN Worcester 18 Experimental Results

  19. On-Line Testing Setup courtesy of GKN Worcester 19 Experimental Results

  20. On-Line Testing: Processing  Processing of individual parts  Profiles have very similar shapes  Some difference due to Part1 having a different angle when manufactured 20 Experimental Results

  21. On-Line Testing: Processing 345 340 Temperature (Degree K) 335 330 325 320 315 310 305 300 0 5 10 15 20 25 30 35 Time (sec) Monitoring the temperature of a spot in the production line 21 Experimental Results

  22. On-Line Testing: Processing 345 340 335 330 Temperature (Degree K) 325 320 315 310 305 300 1 1.2 1.4 1.6 1.8 2 2.2 Time (sec) Monitoring the temperature of a spot in the production line and zooming in one part 22 Experimental Results

  23. On-Line Testing: Discussion  After processing valuable information about the part integrity and quality is available in real time  Process variations causing density gradients can be flagged  Part orientation in the line can be detected  Easy to implement with low cost and space overhead 23 Experimental Results

  24. Accomplishments  Developed an analytical foundation of heating with direct current (electrostatics and heat transfer) and IR detection  Built a suitable model for predicting the thermal profile on the surface of a part ( close to what the IR camera will capture)  Conducted simple dynamic testing of controlled samples with subsurface defects  Conducted on-line testing of simple parts 24 Accomplishments

  25. Future Work  Experimental measurements (Controlled samples)  Different powder mixture  Different compaction densities  Different lubricants and concentrations  Glass and plastic inserts to simulate subsurface defects  Instrumentation efforts  Current strength and pulse shape  Injection methods  Post processing options  Include in the numerical model  Radiation computations  Density variation and non-uniformity  Contact resistance (material parameters) 25 Future Work

  26. Questions 26

  27. Questions 27

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